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In September 2005, radar cross section (RCS) measurements were made of resistive sheets, or R-cards, wrapped around a polystyrene foam cylinder to compare with a newly developed theoretical RCS prediction technique. The resistivities of the R-cards were initially measured with a direct current (DC) four-point probe. When the RCS measurements were compared to the theoretical predictions, it became clear that DC resistivity alone is not sufficient to accurately predict the scattering from an R-card. This thesis presents alternating current (AC) methods for determining the resistivity of an Rcard. Both free-space and waveguide techniques are presented.